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Purifications were conducted by preparative RP-HPLC, eluting with a linear gradient (20 ml min −1 ) and using a binary solvent system consisting of H 2 O:MeCN:TFA (buffer A, 95:5:0.1

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doi: 10.1016/j.bmc.2013.09.016 72 DruceMRMinnionJSFieldBCPatelSRShillitoJCTilbyMet al